HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 71093778, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 71093731 | HCID 71093731 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71093778 | HCID 71093778 | — |
Reaction Steps
The title compound is prepared from 4-{cyclopropyl-[6-(4-methanesulfonyl-phenyl)-pyridine-3-carbonyl]-amino}-piperidine-1-carboxylic acid tert-butyl ester by treatment with trifluoroacetic acid in dichloromethane. LC (method 6): tR=0.70 min; Mass spectrum (ESI+): m/z=400 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921398B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-c9608d2d4e0e4260888f410276484c7b |
| Source note | uspto-grants-2014_12 |