HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanoacetic acid → HCID 178511190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanoacetic acid | HCID 9740 | — |
| Reactant | HCID 178478713 | HCID 178478713 | — |
| Product | HCID 178511190 | HCID 178511190 | — |
Reaction Steps
The title compound, off-white solid (50 mg, 51%), MS (ISP) m/z=394.3 [(M+H)+], mp 186° C., was prepared in accordance with the general method of example 1 from trans-4-[2-(4-benzofuran-3-yl-piperidin-1-yl)-ethyl]-cyclohexylamine dihydrochloride (intermediate A) (100 mg, 0.25 mmol) and 2-cyano-acetic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921397B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-398fc3d774ce4e32863f51e01552c756 |
| Source note | uspto-grants-2014_12 |