HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → HCID 178427473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | HCID 178478713 | HCID 178478713 | — |
| Product | HCID 178427473 | HCID 178427473 | — |
Reaction Steps
The title compound, light brown solid (79 mg, 66%), MS (ISP) m/z=481.3 [(M+H)+], mp 149° C., was prepared in accordance with the general method of example 36 from trans-4-[2-(4-benzofuran-3-yl-piperidin-1-yl)-ethyl]-cyclohexylamine dihydrochloride (intermediate A) (100 mg, 0.25 mmol) and p-toluenesulfonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921397B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-ee6fd21d17074162ab0f89cdf66bf0b8 |
| Source note | uspto-grants-2014_12 |