HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4,4-Trifluorobutanoic acid → HCID 178520632, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4,4-Trifluorobutanoic acid | HCID 2777085 | — |
| Reactant | HCID 178478713 | HCID 178478713 | — |
| Product | HCID 178520632 | HCID 178520632 | — |
Reaction Steps
The title compound, light brown solid (80 mg, 71%), MS (ISP) m/z=451.2 [(M+H)+], mp 192° C., was prepared in accordance with the general method of example 1 from trans-4-[2-(4-benzofuran-3-yl-piperidin-1-yl)-ethyl]-cyclohexylamine dihydrochloride (intermediate A) (100 mg, 0.25 mmol) and 4,4,4-trifluoro-butanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921397B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-2c112e25942f4cee97d9e6d57632773d |
| Source note | uspto-grants-2014_12 |