HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Methanesulfonylthiophene-2-carboxylic acid → HCID 178504774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Methanesulfonylthiophene-2-carboxylic acid | HCID 2740497 | — |
| Reactant | HCID 178478713 | HCID 178478713 | — |
| Product | HCID 178504774 | HCID 178504774 | — |
Reaction Steps
The title compound, yellow solid (101 mg, 78%), MS (ISP) m/z=515.3 [(M+H)+], mp 214° C., was prepared in accordance with the general method of example 1 from trans-4-[2-(4-benzofuran-3-yl-piperidin-1-yl)-ethyl]-cyclohexylamine dihydrochloride (intermediate A) (100 mg, 0.25 mmol) and 5-methanesulfonyl-thiophene-2-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921397B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-303b8e2aaf994b10a34a7b9c9477add3 |
| Source note | uspto-grants-2014_12 |