2,4-Dichlorobenzoic Acid → HCID 178523646, compound

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Reaction Steps

The title compound, light yellow solid (88 mg, 70%), MS (ISP) m/z=499.3 [(M+H)+], mp 187° C., was prepared in accordance with the general method of example 1 from trans-4-[2-(4-benzofuran-3-yl-piperidin-1-yl)-ethyl]-cyclohexylamine dihydrochloride (intermediate A) (100 mg, 0.25 mmol) and 2,4-dichloro-benzoic acid.

Provenance & Evidence