HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86676523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 71250253 | HCID 71250253 | — |
| Product | HCID 86676523 | HCID 86676523 | 100% |
Reaction Steps
A solution of the lysine derivative 9 (174 mg, 0.44 mmol) in TFA (1.4 mL) was stirred at room temperature for 45 minutes and then evaporated in vacuo. The residue was co-evaporated four times with MeOH (4×5 mL) and to give the title compound 10 (160 mg, ˜100%) as a brown oil that was used in the subsequent biochemical studies without any further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08921571B2 |
| Source dataset | uspto-grants-2014_12 |
| ORD ID | ord-c53fa0326aa94956b8410e3ca6ec07c1 |
| Source note | uspto-grants-2014_12 |