Methacrylic Acid → HCID 12764104, compound

HRID 1413128Notes

Reaction equation

HRID 1413128 reaction equation
[C:1]([OH:5])(=[S:4])[CH2:2][CH3:3].[C:6]([OH:11])(=[O:10])[C:7]([CH3:9])=[CH2:8]>>[C:1]([S:4][CH2:8][CH:7]([CH3:9])[C:6]([OH:11])=[O:10])(=[O:5])[CH2:2][CH3:3]

Participants

3

Reactant 2

HCID 4093Methacrylic AcidHCID 178460587HCID 178460587, compound

Product 1

HCID 12764104HCID 12764104, compound

Procedure

A mixture of thiopropanoic acid (50 g) and methacrylic acid (34.1 g) was heated on a steam bath for 3 hours and allowed to stand at room temperature overnight. The reaction mixture was distilled under reduced pressure to give the title compound, b.p. 135°-138° C. (2 mmHg).

Workup

  1. temperaturewas heated on a steam bath for 3 hours
  2. distillationThe reaction mixture was distilled under reduced pressure

Sources & evidence

ORD record
ord-f383120cabc741ac9ff88146e9ec88fd
Source dataset
uspto-grants-1981_02
Patent number
US04248883

Reaction notes

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