HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Aminomethyl-1-ethylpyrrolidine → HCID 20293650, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Aminomethyl-1-ethylpyrrolidine | HCID 117295 | — |
| Edukt | 7-Ethylsulfonyl-1,4-benzodioxane-5-carbonyl chloride | HCID 20544728 | — |
| Produkt | HCID 20293650 | HCID 20293650 | 69,8% |
Reaktionsschritte
In a similar manner 64.5 g of dextrorotary-1-ethyl-2-aminomethylpyrrolidine was reacted with 146 g of 7-ethylsulfonyl-1,4-benzodioxane-5-carbonyl chloride to give, after treatment and purification, 133.5 g of dextrorotatory N-(1-ethyl-2-pyrrolidylmethyl)-7-ethylsulfonyl-1,4-benzodioxane-5-carboxamide (M.P.: 111°-112° C.; yield: 69.8%); (α)D20 =55.5° (in 5% solution in dimethylformamide).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04248885 |
| Quelldatensatz | uspto-grants-1981_02 |
| ORD ID | ord-4ea498dbfb854b9fa9e5efd4ea6e8bce |
| Quellennotiz | uspto-grants-1981_02 |