Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Salicylamide → 2-Propoxybenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Salicylamide | HCID 5147 | — |
| 반응물 | 1-Iodopropane | HCID 33643 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-Propoxybenzamide | HCID 43051 | — |
반응 단계
A 130 gm. portion of salicylamide in 500 ml. of ethanol is reacted with 52.4 gm. of sodium methoxide and 164.9 gm. of 1-iodopropane by heating at reflux. The mixture is cooled, precipitated in 1500 ml. of water and the solid is recrystallized from hot ethanol giving o-propoxybenzamide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | USRE030511 |
| 출처 데이터셋 | uspto-grants-1981_02 |
| ORD ID | ord-54406c68a1c64b7fa2be4b95cccfd99a |
| 출처 메모 | uspto-grants-1981_02 |