Hydrazinecarboxylic acid, ethyl ester → HCID 178473580, compound

HRID 1413271Notes

Reaction equation

HRID 1413271 reaction equation
[C:1]([C:5]1[NH:6][CH:7]=[C:8]([CH:10]=O)[N:9]=1)([CH3:4])([CH3:3])[CH3:2].[C:12]([O:16][CH2:17][CH3:18])(=[O:15])[NH:13][NH2:14]>C(O)C>[CH2:17]([O:16][C:12](=[O:15])[NH:13][N:14]=[CH:10][C:8]1[N:9]=[C:5]([C:1]([CH3:2])([CH3:3])[CH3:4])[NH:6][CH:7]=1)[CH3:18]

Participants

4

Reactant 2

HCID 20064Hydrazinecarboxylic acid, ethyl esterHCID 178441764HCID 178441764, compound

Product 1

HCID 178473580HCID 178473580, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

A 7.6 gm. portion of 2-tert-butyl-4-imidazolecarboxaldehyde and 5.2 gm. of ethyl carbazate in 100 ml. of ethanol are reacted as described in Example 32 giving the desired product, m.p. 194°-197° C.

Sources & evidence

ORD record
ord-b571da2d90404b599c7c14bf001afc83
Source dataset
uspto-grants-1981_02
Patent number
USRE030511

Reaction notes

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