Hydrazinecarboxylic acid, ethyl ester → HCID 136067031, compound

HRID 1413276Notes

Reaction equation

HRID 1413276 reaction equation
[C:1]([C:5]1[NH:6][C:7]([CH3:12])=[C:8]([CH:10]=O)[N:9]=1)([CH3:4])([CH3:3])[CH3:2].[C:13]([O:17][CH2:18][CH3:19])(=[O:16])[NH:14][NH2:15]>>[CH2:18]([O:17][C:13](=[O:16])[NH:14][N:15]=[CH:10][C:8]1[N:9]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[NH:6][C:7]=1[CH3:12])[CH3:19]

Participants

3

Reactant 2

HCID 20064Hydrazinecarboxylic acid, ethyl esterHCID 124932852-(1,1-Dimethylethyl)-4-methyl-1H-imidazole-5-carboxaldehyde

Product 1

HCID 136067031HCID 136067031, compound

Procedure

A 6.17 gm. portion of 2-tert-butyl-5-methyl-4-imidazolecarboxaldehyde and 4.20 gm. of ethyl carbazate are reacted as described in Example 32 giving the desired product, m.p. 226°-228.5° C.

Sources & evidence

ORD record
ord-92d84fd45f5f4e448184fa8059eb11de
Source dataset
uspto-grants-1981_02
Patent number
USRE030511

Reaction notes

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