Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | HCID 20291409 | HCID 20291409 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20291401 | HCID 20291401 | 91.7% |
Reaction Steps
A mixture of 5-methyl-2-(p-nitrophenyl)-4-imidazole methanol (2.9 g, 0.012 mole) and 70% nitric acid (20 ml) is stirred at 50° C. for 3 hours, followed by dilution with water and neutralization with base. The precipitated yellow solid is collected by filtration to yield 2.4 g. (0.011 mole) of title product, dec >270° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | USRE030511 |
|---|
| Source dataset | uspto-grants-1981_02 |
|---|
| ORD ID | ord-85f1fad37e264f5180240029da835e6d |
|---|
| Source note | uspto-grants-1981_02 |
|---|
