HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl carbazate → HCID 136388419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl carbazate | HCID 80519 | — |
| Reactant | 4-Methyl-2-(3-methylphenyl)-1H-imidazole-5-carboxaldehyde | HCID 22411998 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 136388419 | HCID 136388419 | — |
Reaction Steps
A mixture of 5-methyl-2-m-tolyl-4-imidazolecarboxaldehyde (6.9 l g, 0.034 mole), methyl carbazate (3.1 g, 0.034 mole). methylene chloride (70 ml) and acetic acid (1 drop) is refluxed for 1 hour. The precipitated white solid is collected by filtration to yield 7.1 g (0.026 mole), mp. 162°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE030511 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-2861b5892a684987881acb9619fd7d84 |
| Source note | uspto-grants-1981_02 |