Chloroacetic Acid → HCID 86737485, compound

HRID 1413446Notes

Reaction equation

HRID 1413446 reaction equation
ClCC(O)=O.O.[Pt+2:7].[CH2:8]([NH:10][CH2:11][CH2:12][NH:13][CH2:14][CH3:15])[CH3:9].[K]>>[Pt+2:7].[CH2:8]([NH:10][CH2:11][CH2:12][NH:13][CH2:14][CH3:15])[CH3:9]

Participants

4

Reactant 3

HCID 300Chloroacetic AcidHCID 5462222PotassiumHCID 86737486HCID 86737486, compound

Product 1

HCID 86737485HCID 86737485, compound

Procedure

Chloroacetic acid (19.4 g, 0.205 mol) was added to a stirred solution of the N-ethylethylenediamine diaquo complex (0.92 mol). The solution was adjusted to pH 5-6 with potassium hydoroxide, and then warmed to give a pale yellow precipitate. The mixture was stirred overnight and the solid filtered off, washed with water (20 ml), ethanol (25 ml) and dried in vacuo at 60° C. for four hours.

Workup

  1. temperaturewarmed
  2. customto give a pale yellow precipitate
  3. filtrationthe solid filtered off
  4. washwashed with water (20 ml), ethanol (25 ml)
  5. customdried in vacuo at 60° C. for four hours

Sources & evidence

ORD record
ord-78b8c039f5834be09a54ab49cc1583a8
Source dataset
uspto-grants-1981_02
Patent number
US04250189

Reaction notes

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