9H-xanthene-9-carbonyl chloride → HCID 15572560, compound

HRID 1413546Notes

Reaction equation

HRID 1413546 reaction equation
[CH2:1]([N:4]1[CH2:9][CH2:8][N:7]([CH2:10][CH2:11][CH2:12][OH:13])[CH2:6][CH2:5]1)[CH:2]=[CH2:3].[CH:14]1[C:27]2[CH:26]([C:28]([Cl:30])=[O:29])[C:25]3[C:20](=[CH:21][CH:22]=[CH:23][CH:24]=3)[O:19][C:18]=2[CH:17]=[CH:16][CH:15]=1>>[ClH:30].[ClH:30].[CH2:1]([N:4]1[CH2:9][CH2:8][N:7]([CH2:10][CH2:11][CH2:12][O:13][C:28]([CH:26]2[C:27]3[CH:14]=[CH:15][CH:16]=[CH:17][C:18]=3[O:19][C:20]3[C:25]2=[CH:24][CH:23]=[CH:22][CH:21]=3)=[O:29])[CH2:6][CH2:5]1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 27608929H-xanthene-9-carbonyl chlorideHCID 15572524HCID 15572524, compound

Product 1

HCID 15572560HCID 15572560, compoundYield 76%

Procedure

3-(4-Allyl-piperazin-1-yl)-hydroxy-propane, prepared as described in Example 2, Step A, is reacted with xanthene-9-carbonyl chloride as described in Example 1, Step B. 3-(4-Allyl-piperazin-1-yl)-1-(xanthene-9-carbonyloxy)-propane dihydrochloride is obtained with a yield of 76%; m.p.: 209°-211° C.

Sources & evidence

ORD record
ord-39f50c530c6d4885a0082aad91afbbe2
Source dataset
uspto-grants-1981_02
Patent number
US04250310

Reaction notes

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