HuagongsheHuagongshe Chemistry Print Report · For research reference only
Picolyl chloride hydrochloride → N-Cyano-N'-(2-propyn-1-yl)-N"-{2-[(2-pyridyl)methylthio]ethyl}guanidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Picolyl chloride hydrochloride | HCID 23392 | — |
| Reactant | N-Cyano-N'-propargyl-N"-(2-mercaptoethyl)guanidine | HCID 136182246 | — |
| Product | N-Cyano-N'-(2-propyn-1-yl)-N"-{2-[(2-pyridyl)methylthio]ethyl}guanidine | HCID 136023173 | — |
Reaction Steps
The ethanolic solution of the product of Step A is reacted with about an equimolar amount of 2-chloromethylpyridine hydrochloride and about two equivalents of base to produce the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04250316 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-7c45144647d4438ab4719ba3966b024b |
| Source note | uspto-grants-1981_02 |