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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1413567Generated: November 2, 2026

Water → Methyl Acetate

https://huagongshe.com/reaction/1413567

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantTerephthalic AcidHCID 7489—
ReactantP-XyleneHCID 7809—
ReactantBromineHCID 24408—
CatalystCobaltHCID 104730—
SolventAcetic AcidHCID 176—
ProductMethyl AcetateHCID 6584—
ProductTerephthalic AcidHCID 7489—

Reaction Steps

In a process for the synthesis of terephthalic acid, comprising the oxidation of para-xylene in acetic acid solution, at a temperature of from 100° to 230° C. and at a pressure from 1 to 30 kg/cm2, and in the presence of a catalytic system based on manganese, bromine and cobalt, whereby water is formed and methyl-acetate is by-produced during the oxidation, whereby solid terephthalic acid is separated from the mother liquor and whereby one withdraws from the oxidation zone a liquid which is obtained by condensing the vapors released during the oxidation and which are mainly consisting of acetic acid and water, the improvement for the recovery of the acetic acid solvent, the catalyst and the methyl acetate, comprising:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04250330
Source datasetuspto-grants-1981_02
ORD IDord-2a2d77e2d5cf4ca8b33728f5a92cc925
Source noteuspto-grants-1981_02