HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzoyl chloride → HCID 20292119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzoyl chloride | HCID 8501 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | ethyl [(4-methoxyphenyl)amino]acetate | HCID 6917278 | — |
| Reactant | HCID 20292261 | HCID 20292261 | — |
| Solvent | Benzene | HCID 241 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 20292119 | HCID 20292119 | — |
Reaction Steps
Ethyl p-anisidinoacetate is dissolved in an inert solvent (benzene) and is mixed with an equivalent quantity of p-chlorobenzoyl chloride in the presence of an equivalent quantity of pyridine. The resultant ethyl N-(p-chlorobenzoyl)-p-anisidinoacetate is saponified with alcoholic potash to produce N-(p-chlorobenzoyl)-p-anisidinoacetic acid, melting point: 195° to 197°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04250183 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-b5ef4a453cef4c7ab044142a1de37abe |
| Source note | uspto-grants-1981_02 |