HuagongsheHuagongshe Chemistry Print Report · For research reference only
Clanobutin → ethyl N-[N-(p-chlorobenzoyl)-4-(p-anisidino)butyryl]-4-(2,6-dimethylanilino)butyrate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Clanobutin | HCID 35378 | — |
| Reactant | Ethyl 4-(2,6-dimethylanilino)butyrate | HCID 20292063 | — |
| Product | ethyl N-[N-(p-chlorobenzoyl)-4-(p-anisidino)butyryl]-4-(2,6-dimethylanilino)butyrate | HCID 20292148 | — |
Reaction Steps
Analogously to Example 1, by using equivalent quantities, reacting N-(p-chlorobenzoyl)-4-(p-anisidino)-butyric acid and ethyl 4-(2,6-dimethylanilino)butyrate and suitable processing produces ethyl N-[N-(p-chlorobenzoyl)-4-(p-anisidino)butyryl]-4-(2,6-dimethylanilino)butyrate (oil), saponification of which and the processing of the reaction product yields N-[N-(p-chlorobenzoyl)-4-(p-anisidino)butyryl]-4-(2,6-dimethylanilino)butyric acid (M.P. 131° to 133°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04250183 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-6dd7f7646b4c4b45ae7fb5edd6b59eb8 |
| Source note | uspto-grants-1981_02 |