HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyric acid, 4-(p-chloro-N-2,6-xylylbenzamido)- → HCID 22814603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyric acid, 4-(p-chloro-N-2,6-xylylbenzamido)- | HCID 35383 | — |
| Reactant | L-Alanine methyl ester | HCID 82335 | — |
| Product | HCID 22814603 | HCID 22814603 | — |
Reaction Steps
Analogously to Example 1, by using equivalent quantities, reacting N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyric acid and methyl L-alaninate and suitable processing produces methyl N-[N-(p-chlorobenzoyl)-4-(2,6dimethylanilino)butyryl]-L-alaninate (M.P. 91° to 92°), saponification of which and processing of the reaction product yields N-[N-(p-chlorobenzoyl)-4-(2,6-dimethylanilino)butyryl]-L-alanine (M.P. 159° to 161°).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04250183 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-ee1dc04540464853bfcc9edf947574eb |
| Source note | uspto-grants-1981_02 |