Potassium Hydroxide → HCID 20292245, compound

HRID 1413614Notes

Reaction equation

HRID 1413614 reaction equation
COC1C=C(C=C(OC)C=1OC)C(N(C(C)(C)C)CCCCCC(O)=O)=O.[CH3:28][O:29][C:30]1[CH:35]=[CH:34][C:33]([NH:36][CH2:37][CH2:38][CH2:39][C:40]([O:42]CC)=[O:41])=[CH:32][CH:31]=1.[OH-].[K+]>C(O)C>[CH3:28][O:29][C:30]1[CH:31]=[CH:32][C:33]([NH:36][CH2:37][CH2:38][CH2:39][C:40]([OH:42])=[O:41])=[CH:34][CH:35]=1

Participants

5

Reactant 3

HCID 14797Potassium HydroxideHCID 20292202HCID 20292202, compoundHCID 20292215HCID 20292215, compound

Product 1

HCID 20292245HCID 20292245, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Analogously to Example 1, by using equivalent quantities, reacting N-(3,4,5-trimethoxybenzoyl)-6-(tert.-butylamino)caproic acid and ethyl γ-(p-anisidino)butyrate and suitable processing, dissolving the evaporation residue in ethanol, adding an ethanolic solution of potassium hydroxide, stirring for 12 hours at room temperature and further processing yields N-[N-(3,4,5-trimethoxybenzoyl)-6-tert.-butylamino)hexanoyl]-4-(p-anisidino)butyric acid.

Sources & evidence

ORD record
ord-d2b7c6183565442f8484c65fa2d7adfb
Source dataset
uspto-grants-1981_02
Patent number
US04250183

Reaction notes

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