Diallylamine → HCID 20290268, compound

HRID 1413650Notes

Reaction equation

HRID 1413650 reaction equation
[CH2:1]([NH:4][CH2:5][CH:6]=[CH2:7])[CH:2]=[CH2:3].[F:8][C:9]([F:27])([F:26])[C:10]1[CH:11]=[C:12]([CH:23]=[CH:24][CH:25]=1)[O:13][C:14]1[N:22]=[CH:21][CH:20]=[CH:19][C:15]=1[C:16](Cl)=[O:17]>C1C=CC=CC=1>[F:8][C:9]([F:27])([F:26])[C:10]1[CH:11]=[C:12]([CH:23]=[CH:24][CH:25]=1)[O:13][C:14]1[N:22]=[CH:21][CH:20]=[CH:19][C:15]=1[C:16]([N:4]([CH2:5][CH:6]=[CH2:7])[CH2:1][CH:2]=[CH2:3])=[O:17]

Participants

4

Reactant 2

HCID 31279DiallylamineHCID 111624242-(3-Trifluoromethylphenoxy)nicotinoyl chloride

Product 1

HCID 20290268HCID 20290268, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

In the same manner as in Example 1(a), 1.6 grams (0.016 mole) diallylamine and 2.5 grams (0.008 mole) 2-(3-trifluoromethylphenoxy)nicotinoyl chloride were mixed in 100 milliliters benzene to yield 1.6 grams (55.2% of theoretical yield) of the desired product, nD30 1.5003. The structure of this compound was confirmed by mass spectrometry.

Workup

  1. customto yield

Sources & evidence

ORD record
ord-b39d14081c864f9c8a5020e73c56ea86
Source dataset
uspto-grants-1981_02
Patent number
US04251263

Reaction notes

Loading…