HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 12536141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | HCID 12218835 | HCID 12218835 | — |
| Reactant | HCID 53806130 | HCID 53806130 | — |
| Solvent | 1,2-Dichlorobenzene | HCID 7239 | — |
| Product | HCID 12536141 | HCID 12536141 | — |
Reaction Steps
To 15 ml. of o-dichlorobenzene were added 5.8 g. of 2-cyanomethylene-cyclohexane-carboxylic acid ethyl ester, 6.5 g. of 3-aminopropanethiol hydrobromide and 3.1 g. of sodium acetate. Then, by treating the mixture as in Example 95, 800 mg. of 6-oxo-3,4,7,8,9,10-hexahydro-2H,6H-1,3-thiazino[3,2-b]isoquinoline was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04251533 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-31cb9f088d2c4508981bdd854157e6a2 |
| Source note | uspto-grants-1981_02 |