HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → 1-(p-Prenylphenyl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | p-Prenylacetophenone | HCID 11217703 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(p-Prenylphenyl)ethanol | HCID 13217275 | 91.5% |
Reaction Steps
To a solution of 20.0 g of p-prenylacetophenone in 200 ml of methanol, 1.5 g of sodium borohydride was added at 20° C. with stirring. After stirring for 4 hours, 300 ml of water was added, the resulting solution was extracted with ethyl ether. The extract was washed with water, dried, concentrated and distilled to give 18.5 g of 1-(p-prenylphenyl)-ethanol, b.p. 107-108 °C/0.30 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04251543 |
| Source dataset | uspto-grants-1981_02 |
| ORD ID | ord-4bc2ae96455940ebb9b703c423bd48f7 |
| Source note | uspto-grants-1981_02 |