Sodium Hydroxide → HCID 23717791, compound

HRID 1413834Notes

Reaction equation

HRID 1413834 reaction equation
[CH2:1]([C:6]1[CH:11]=[CH:10][C:9]([CH:12]([CH3:16])[C:13]([OH:15])=[O:14])=[CH:8][CH:7]=1)[CH:2]=[C:3]([CH3:5])[CH3:4].[OH-].[Na+:18]>>[CH2:1]([C:6]1[CH:7]=[CH:8][C:9]([CH:12]([CH3:16])[C:13]([O-:15])=[O:14])=[CH:10][CH:11]=1)[CH:2]=[C:3]([CH3:5])[CH3:4].[Na+:18]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 1754602-(4-(3-Methyl-2-butenyl)phenyl)propionic acid

Product 1

HCID 23717791HCID 23717791, compound

Procedure

4.8 g of 2-(p-prenylphenyl)propionic acid as prepared in Example 1 was dissolved in 5% aqueous sodium hydroxide solution to adjust to pH 9.0. After evaporation of the water, the resulting solid was recystallized from ethyl acetate to give 4.5 g of sodium 2-(p-prenylphenyl)propionate, colorless prisms, m.p. 65°-66° C.

Workup

  1. customAfter evaporation of the water

Sources & evidence

ORD record
ord-0ad9b185ceb1465882d6c3bea7e8b5ff
Source dataset
uspto-grants-1981_02
Patent number
US04251543

Reaction notes

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