Cyclobutanecarbonyl chloride → HCID 21486339, compound

HRID 1414186Notes

Reaction equation

[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([N+:11]([O-:13])=[O:12])[CH:3]=1.[CH:14]1([C:18](Cl)=[O:19])[CH2:17][CH2:16][CH2:15]1>>[CH:14]1([C:18]([NH:1][C:2]2[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([N+:11]([O-:13])=[O:12])[CH:3]=2)=[O:19])[CH2:17][CH2:16][CH2:15]1

Participants

Reactant 2

HCID 78705Cyclobutanecarbonyl chloride

HCID 2357134-Amino-2-nitrobenzoic Acid

Product 1

HCID 21486339HCID 21486339, compound

Procedure

B 4-Cyclobutanecarbonylamino-2-nitro-benzoic acid was prepared as described in Example 3 from 10.9 g (0.06 mol) of 4-amino-2-nitro-benzoic acid and 7.83 g (0.066 mol) of cyclobutanecarboxylic acid chloride.

Sources & evidence

ORD record: ord-3ec4e6e4126543c697f4a51e622f2c86
Source dataset: uspto-grants-1977_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04001218

Reaction notes

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