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HRID1414195

反应详情

EQUATION

反应方程式

HRID 1414195 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)c1ccc([N+](=O)[O-])cc1
HCID8502

4-Nitrobenzoyl chloride

C7H4ClNO3

结构：Nc1ccc(C(=O)O)c([N+](=O)[O-])c1
HCID235713

4-amino-2-nitrobenzoic acid

C7H6N2O4

PRODUCTS

生成物

1
结构：O=C(Nc1ccc(C(=O)O)c([N+](=O)[O-])c1)c1ccc([N+](=O)[O-])cc1
HCID21486331

未命名化合物

PROCEDURE

实验过程

4-(4-Nitrobenzoylamino)-2-nitrobenzoic acid was prepared as described in Example 3 from 20.0 g (0.11 mol) of 4-amino-2-nitrobenzoic acid and 22.4 g (0.121 mol) of 4-nitrobenzoyl chloride. The product was reprecipitated from THF/H2O.

WORKUP

后处理

  1. customThe product was reprecipitated from THF/H2O