HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 21486849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 88082025 | HCID 88082025 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21486849 | HCID 21486849 | — |
Reaction Steps
A mixture of ethyl 1,3,4-oxadiazole-2-thione-5-carboxylate potassium salt dimethylsulfoxide solvate (11 g., 0.03 mole) and ethyl iodide (7 g., 0.045 mole) in absolute ethanol (100 ml.) was heated at reflux for 45 minutes and then worked up as described previously in Experiment A to yield the title compound (5.59 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001238 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-1ade5e5a71b34ee3af5caa1326e1019c |
| Source note | uspto-grants-1977_01 |