Isopropyl iodide → HCID 21486851, compound

HRID 1414235Notes

Reaction equation

HRID 1414235 reaction equation
[K].[O:2]1[C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[N:5][NH:4][C:3]1=[S:12].[CH:13](I)([CH3:15])[CH3:14]>>[CH:13]([S:12][C:3]1[O:2][C:6]([C:7]([O:9][CH2:10][CH3:11])=[O:8])=[N:5][N:4]=1)([CH3:15])[CH3:14]

Participants

3

Procedure

The title compound was prepared from ethyl 1,3,4-oxadiazole-2-thione-5-carboxylate potassium salt dimethylsulfoxide solvate (11 g., 0.03 mole) and isopropyl iodide (5.6 g., 0.03 mole) analogously to the procedure described in Experiment A. The yield was 4.1 g. (63%).

Sources & evidence

ORD record
ord-6d8683111fbd429bb088d56066f9d733
Source dataset
uspto-grants-1977_01
Patent number
US04001238

Reaction notes

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