HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-methoxy-N-methyl-2-(2-pyridyl)thioacetamide hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | alpha-methoxy-N-methyl-2-pyridylthioacetamide | HCID 15581955 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-methoxy-N-methyl-2-(2-pyridyl)thioacetamide hydrochloride | HCID 21486894 | — |
Reaction Steps
2-Methoxy-N-methyl-2-(2-pyridyl)thioacetamide (500 mg.) in ether is added to ethereal hydrogen chloride. The resulting precipitate is filtered off and recrystallized from ethanol/ether to give 2-methoxy-N-methyl-2-(2-pyridyl)thioacetamide hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001241 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-858bc0fadad94b66b6d85d36b3395ed6 |
| Source note | uspto-grants-1977_01 |