HCID 20130167, compound → HCID 70090373, compound

HRID 1414359Notes

Reaction equation

HRID 1414359 reaction equation
[F:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]3[CH:12]=[N:13][N:14]=[C:10]3[CH2:9][N:8]=[C:7]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=3)[C:6]=2[CH:21]=1.[I-].CC(=[NH2+])C>>[F:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]3[CH2:12][N:13]=[N:14][C:10]3=[CH:9][N:8]=[C:7]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][N:16]=3)[C:6]=2[CH:21]=1

Participants

3

Reactant 2

HCID 20130167HCID 20130167, compoundHCID 21487191HCID 21487191, compound

Product 1

HCID 70090373HCID 70090373, compound

Procedure

In manner given in Example 5, 8-fluoro-6-(2-pyridyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine is treated with dimethylmethylene ammonium iodide to give 8-fluoro-6-(2-pyridyl)-s-triazolo[4,3-a][1,4]benzodiazepine.

Sources & evidence

ORD record
ord-b33a14dce3ae424da48e0d126646d625
Source dataset
uspto-grants-1977_01
Patent number
US04001262

Reaction notes

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