Benzylamine → HCID 21487297, compound

HRID 1414395Notes

Reaction equation

HRID 1414395 reaction equation
O1C=CC=C1C[NH:7][C:8]1[C:9](=[CH:13][C:14]([S:25](=[O:28])(=[O:27])[NH2:26])=[C:15]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([Cl:24])[CH:19]=2)[CH:16]=1)[C:10]([OH:12])=[O:11].[CH2:29]([NH2:36])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[CH2:29]([NH:36][NH:7][C:8]1[C:9](=[CH:13][C:14]([S:25](=[O:27])(=[O:28])[NH2:26])=[C:15]([O:17][C:18]2[CH:23]=[CH:22][CH:21]=[C:20]([Cl:24])[CH:19]=2)[CH:16]=1)[C:10]([OH:12])=[O:11])[C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 21487301HCID 21487301, compound

Product 1

HCID 21487297HCID 21487297, compound

Procedure

45.5 g of the carboxylic acid prepared in Example 9 (b) (0.1 mol) were reacted with 100 ml of benzylamine as in Example 9 (c), and the reaction product was purified by recrystallization from ethanol.

Workup

  1. customthe reaction product was purified by recrystallization from ethanol

Sources & evidence

ORD record
ord-26bc100085c34a1981b3bb28f0faec69
Source dataset
uspto-grants-1977_01
Patent number
US04001284

Reaction notes

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