2-Naphthalenethiol → HCID 68125195, compound
Reaction equation
[CH:1]1[CH:10]=[C:9]2[C:4]([CH:5]=[C:6]([SH:11])[CH:7]=[CH:8]2)=[CH:3][CH:2]=1.Br[CH2:13][CH:14]=[C:15]([CH3:22])[CH2:16][CH2:17][CH:18]=[C:19]([CH3:21])[CH3:20]>>[CH:5]1[C:4]2[C:9](=[CH:10][CH:1]=[CH:2][CH:3]=2)[CH:8]=[CH:7][C:6]=1[S:11][CH2:13][CH:14]=[C:15]([CH3:22])[CH2:16][CH2:17][CH:18]=[C:19]([CH3:21])[CH3:20]Participants
3
Procedure
2-thionaphthol is reacted with 1-bromo-3,7-dimethyl-octa-2,6-diene to produce 3,7-dimethyl-octa-2,6-dienyl 2-naphthyl sulphide (boiling point = 138° C/0.25 mmHg;
Sources & evidence
- ORD record
- ord-de424cd75eec4f778206f9ddc9d68118
- Source dataset
- uspto-grants-1977_01
- Patent number
- US04001339
Reaction notes
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