Diisobutylamine → p-[(1,5-dimethyl-hexyl)-oxy]-N,N-diisobutylbenzamide
Reaction equation
[CH2:1]([NH:5][CH2:6][CH:7]([CH3:9])[CH3:8])[CH:2]([CH3:4])[CH3:3].CO[C:12](=[O:28])[C:13]1[CH:18]=[CH:17][C:16]([O:19][CH:20]([CH3:27])[CH2:21][CH2:22][CH2:23][CH:24]([CH3:26])[CH3:25])=[CH:15][CH:14]=1>>[CH3:27][CH:20]([O:19][C:16]1[CH:15]=[CH:14][C:13]([C:12]([N:5]([CH2:6][CH:7]([CH3:9])[CH3:8])[CH2:1][CH:2]([CH3:4])[CH3:3])=[O:28])=[CH:18][CH:17]=1)[CH2:21][CH2:22][CH2:23][CH:24]([CH3:25])[CH3:26]Participants
3
Procedure
By the procedure given in Example 47, diisobutylamine is reacted with p-[(1,5-dimethyl-hexyl)-oxy]-benzoic acid methyl ester to produce p-[(1,5-dimethyl-hexyl)-oxy]-N,N-diisobutylbenzamide (nD24 = 1.4968).
Sources & evidence
- ORD record
- ord-ab23b6146dc2428f8dc70033f16a822a
- Source dataset
- uspto-grants-1977_01
- Patent number
- US04001339
Reaction notes
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