HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Chlorobutyl)-1-Ethyl-7-Methoxy-2-Tetralone → 5-Ethyl-6,7,8,9,10,11-Hexahydro-3-Methoxy-5,10-Methano-5H-Benzocyclononen-12-One
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Chlorobutyl)-1-Ethyl-7-Methoxy-2-Tetralone | HCID 21410117 | — |
| Reactant | 6,7,8,9,10,11-hexahydro-3-methoxy-5-methyl-5,10-methano-5H-benzocyclononen 12-one | HCID 21410123 | — |
| Product | 5-Ethyl-6,7,8,9,10,11-Hexahydro-3-Methoxy-5,10-Methano-5H-Benzocyclononen-12-One | HCID 21410072 | — |
Reaction Steps
Using a procedure analogous to that described in Example X for the preparation of 6,7,8,9,10,11-hexahydro-3-methoxy-5-methyl-5,10-methano-5H-benzocyclononen-12-one there is obtained from 37.4 g. of 1-(4-chlorobutyl)-1-ethyl-7-methoxy-2-tetralone, 22.2 g. of the title product, b.p. 138° to 142° C. (0.35 mm.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04001326 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-cca0321c02f247e7955ed792508d89ce |
| Source note | uspto-grants-1977_01 |