HRID1414491
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Using a procedure analogous to that described in Example XXVIIA for the preparation of 6,7,8,9,10,11hexahydro-3-methoxy-5-methyl-5,10-methano-5H-benzocyclononen-12-amine there is obtained from 3.5 g. of 5-ethyl-6,7,8,9,10,11-hexahydro-3-methoxy-5,10-methano-5H-benzocyclononen-12-one, oxime 1.6 g. of the title product, b.p. 150-160° C. (0.5 mm.).
WORKUP
后处理
- customthere is obtained from 3.5 g