3,5-Dimethylbenzoyl Chloride → HCID 21488004, compound

HRID 1414630Notes

Reaction equation

HRID 1414630 reaction equation
[CH3:1][O:2][C:3]1[CH:18]=[CH:17][C:6]([CH2:7][C:8]2[C:12]3[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=3[O:10][CH:9]=2)=[CH:5][CH:4]=1.[CH3:19][C:20]1[CH:21]=[C:22]([CH:26]=[C:27]([CH3:29])[CH:28]=1)[C:23](Cl)=[O:24]>C(Cl)Cl>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([CH2:7][C:8]2[C:12]3[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=3[O:10][C:9]=2[C:23](=[O:24])[C:22]2[CH:26]=[C:27]([CH3:29])[CH:28]=[C:20]([CH3:19])[CH:21]=2)=[CH:17][CH:18]=1

Participants

4

Reactant 2

HCID 810883,5-Dimethylbenzoyl ChlorideHCID 54476131HCID 54476131, compound

Product 1

HCID 21488004HCID 21488004, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Acylation of 3-p-methoxybenzylbenzofuran with 3,5-dimethylbenzoyl chloride and stannic chloride in methylene chloride according to the procedure described in Example 1 gives 3-p-methoxybenzyl-2-(3',5'-dimethylbenzoyl)benzofuran.

Sources & evidence

ORD record
ord-4d2fdec405994830b069ab557eacf5aa
Source dataset
uspto-grants-1977_01
Patent number
US04001426

Reaction notes

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