Sodium Hydroxide → HCID 70590428, compound

HRID 1414672Notes

Reaction equation

HRID 1414672 reaction equation
[OH-].[Na+:2].[CH3:3][S:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[CH:11]=[C:10]([CH:15]([CH3:19])[C:16]([OH:18])=[O:17])[CH:9]=[CH:8]2>CO>[CH3:3][S:4][C:5]1[CH:6]=[C:7]2[C:12](=[CH:13][CH:14]=1)[CH:11]=[C:10]([CH:15]([CH3:19])[C:16]([O-:18])=[O:17])[CH:9]=[CH:8]2.[Na+:2]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 20335119HCID 20335119, compound

Product 1

HCID 70590428HCID 70590428, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Conditions

Temperature
50 °C

Procedure

To a mixture of 4 g. of sodium hydroxide and 500 ml. of methanol are added 24.6 g. of 6-methylthio-2-naphthyl-α-methylacetic acid. The mixture is stirred for 18 hours at 50° C. The cooled mixture is then evaporated to give sodium 6-methylthio-2-naphthyl-α-methylacetate.

Workup

  1. additionTo a mixture of 4 g
  2. customThe cooled mixture is then evaporated

Sources & evidence

ORD record
ord-653739e45962434c8d2c8cf31d62764d
Source dataset
uspto-grants-1977_01
Patent number
US04001301

Reaction notes

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