HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Phenylenediamine → HCID 21484692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Phenylenediamine | HCID 7935 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Terephthalic acid monomethylester chloride | HCID 53442854 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 21484692 | HCID 21484692 | — |
Reaction Steps
The following are reacted in accordance with the instruction given in Example A: 180 g of terephthalic acid monomethyl ester monochloride (0.9 mol) dissolved in 1.8 liters of benzene, with 48.6 g of m-phenylenediamine (0.45 mol) and 126 ml of triethylamine in a mixture of 450 ml of benzene and 450 ml of acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002600 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-fd3d8ccb842a4d218810389ade5b6133 |
| Source note | uspto-grants-1977_01 |