HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → 6-Nitroveratrylideneallylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 6-Nitroveratraldehyde | HCID 88505 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 6-Nitroveratrylideneallylamine | HCID 86733611 | 99.9% |
Reaction Steps
A suspension of 6-nitroveratraldehyde (84 g, 0.4 mole) and ethanol (1200 ml) was refluxed with a solution of allylamine (21 g, 0.44 mole) and ethanol (100 ml) for 1.5 hrs. The resulting dark solution was concentrated to dryness in vacuo leaving 100 g of a dark oil which solidified.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002652 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-b5fb7310d6e345518eb3f7d8b1bf31bf |
| Source note | uspto-grants-1977_01 |