HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 13860722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 5-Chloro-2-nitroaniline | HCID 74218 | — |
| Reactant | Benzenesulfinic acid, sodium salt | HCID 2723840 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13860722 | HCID 13860722 | — |
Reaction Steps
2.0 g. of 2 amino-4-chloro-1-nitrobenzene and 5.0 g. sodium benzene-sulfinate in 20 ml. dimethylformamide is heated at reflux for 3 hours. The mixture is cooled, diluted with water and the product filtered off to give 2-amino-1-nitro-4-phenylsulfonylbenzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002640 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-a7b931c682a64860b4cb5ce803b1e76a |
| Source note | uspto-grants-1977_01 |