HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → 4-[(Methoxymethyl)sulfanyl]-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-{4-[(Methoxymethyl)sulfanyl]-2-nitrophenyl}acetamide | HCID 20362834 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-[(Methoxymethyl)sulfanyl]-2-nitroaniline | HCID 20362817 | — |
Reaction Steps
1.4 G. of 1-acetamido-2-nitro-4-methoxymethylthiobenzene is treated with 3 ml. 5N sodium hydroxide and 6 ml. methanol in the steam bath for about 15 minutes. The mixture is stripped under vacuum and the residue extracted with chloroform. The dried extracts are evaporated giving 1-amino-2-nitro-4-methoxymethylthiobenzene as a red crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002640 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-67db31d7185746f0beb7c391386d6ea0 |
| Source note | uspto-grants-1977_01 |