HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Methoxymethoxy)-2-nitroaniline → 4-(Methoxymethoxy)benzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Methoxymethoxy)-2-nitroaniline | HCID 18509202 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(Methoxymethoxy)benzene-1,2-diamine | HCID 20362822 | — |
Reaction Steps
A mixture of 3.5 g. of 2-nitro-4-methoxymethoxyaniline, 1 g. of 5% palladium-on-charcoal catalyst and 120 ml. of methanol is hydrogenated at ambient conditions. After the uptake of hydrogen is complete, the mixture is filtered and 1,2-diamino-4-methoxymethoxybenzene is obtained by evaporation of the solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002640 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-460d0990721649d9869c1ff510d2bd89 |
| Source note | uspto-grants-1977_01 |