HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Ethoxyethoxy)-2-nitroaniline → 4-(2-Ethoxyethoxy)benzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Ethoxyethoxy)-2-nitroaniline | HCID 20362808 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(2-Ethoxyethoxy)benzene-1,2-diamine | HCID 54492542 | — |
Reaction Steps
A mixture of 1.8 g. of 4-(2-ethoxyethoxy)-2-nitroaniline and 0.3 g. of 5% palladium-on-charcoal catalyst in 200 ml. of methanol is hydrogenated under ambient conditions. After the uptake of hydrogen is complete, the mixture is filtered and 1,2-diamino-4-(2-ethoxyethoxy) benzene is isolated from the filtrate by evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002640 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-1f3813fbe62f4fb687594032b46b5e82 |
| Source note | uspto-grants-1977_01 |