HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dihydro-1-benzofuran-6-ol → 6-[(3,7-Dimethyloct-6-EN-1-YL)oxy]-2,3-dihydro-1-benzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dihydro-1-benzofuran-6-ol | HCID 12236540 | — |
| Reactant | 3,7-Dimethyl-6-octenyl p-toluenesulfonate | HCID 14149791 | — |
| Product | 6-[(3,7-Dimethyloct-6-EN-1-YL)oxy]-2,3-dihydro-1-benzofuran | HCID 21485115 | — |
Reaction Steps
3,7-dimethyl-6-octenyl p-toluenesulfonate and 6-hydroxy-2,3-dihydrobenzofuran are reacted to produce 6-[(3,7-dimethyl-6-octenyl)-oxy]-2,3-dihydrobenzofuran of boiling point 126°-128° C./0.001 mmHg; nD20 = 1.5223; and 3,7-dimethyl-6-octenyl p-toluenesulfonate and 6-hydroxy-3-methyl-2,3-dihydrobenzofuran are reacted to produce 6-[(3,7-dimethyl-6-octenyl)-oxy]-3-methyl-2,3-dihydrobenzofuran of boiling point (bulb-tube) 130° C./0.14 mmHg; nD20 = 1.5150.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04002647 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-25987cef4bd44e7d86422f1d7861165c |
| Source note | uspto-grants-1977_01 |