HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-(Diethylamino)-2-methylphenol--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | 5-(Ethylamino)-2-methylphenol | HCID 15801248 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(Diethylamino)-2-methylphenol--hydrogen chloride (1/1) | HCID 20376065 | — |
Reaction Steps
5 gm of 5-(ethylamino)-2-methylphenol were dissolved in 50 ml of ethanol, then alkylated analogously to the procedure described in Example 4 with 5,2 gm ethyl bromide, and worked up. The hydrochloride had a melting point of 192° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04003699 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-21ace5bc68634e85ac9c5d52388a8e78 |
| Source note | uspto-grants-1977_01 |