HCID 21483912, compound → HCID 21483919, compound

HRID 1415211Notes

Reaction equation

HRID 1415211 reaction equation
COC1C(Cl)=C(Cl)C2C(=O)CCCCC=2C=1.C[O:18][C:19]1[C:20]([Cl:34])=[C:21]([Cl:33])[C:22]2[C:28](=[O:29])[CH:27]([CH2:30][CH3:31])[CH2:26][CH2:25][CH2:24][C:23]=2[CH:32]=1>>[OH:18][C:19]1[C:20]([Cl:34])=[C:21]([Cl:33])[C:22]2[C:28](=[O:29])[CH:27]([CH2:30][CH3:31])[CH2:26][CH2:25][CH2:24][C:23]=2[CH:32]=1

Participants

3

Reactant 2

HCID 21483912HCID 21483912, compoundHCID 21483922HCID 21483922, compound

Product 1

HCID 21483919HCID 21483919, compound

Procedure

By the process of Example VI, Step 2, but substituting for the 2-methoxy-3,4-dichloro-6,7,8,9-tetrahydro- 5H-benzocyclohepten-5-one used therein an equivalent amount of 2-methoxy-3,4-dichloro-6-ethyl-6,7,8,9-tetrahydro- 5H-benzocyclohepten-5-one and conducting the reaction as described in Example VI, Step 2, there is obtained 2-hydroxy- 3,4-dichloro-6-ethyl-6,7,8,9-tetrahydro-5H-benzocyclohepten- 5-one.

Workup

  1. customthe reaction

Sources & evidence

ORD record
ord-06fc718a10a643078f37423f24903b59
Source dataset
uspto-grants-1977_01
Patent number
US04003927

Reaction notes

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