HCID 86734427, compound → HCID 86734426, compound

HRID 1415269Notes

Reaction equation

HRID 1415269 reaction equation
Cl.[CH3:2][O:3][C:4]1[CH:5]=[C:6]([C:12]2([CH2:22][CH2:23][CH2:24][N:25]([CH3:35])CCC3C=CC(C)=CC=3)[S:17](=[O:19])(=[O:18])[CH2:16][CH2:15][CH2:14][S:13]2(=[O:21])=[O:20])[CH:7]=[CH:8][C:9]=1[O:10][CH3:11]>CC(C)=O.C(OCC)(=O)C>[CH3:2][O:3][C:4]1[CH:5]=[C:6]([C:12]2([CH2:22][CH2:23][CH2:24][NH:25][CH2:35][CH2:23][CH2:22][CH2:12][C:6]3[CH:7]=[CH:8][C:9]([O:10][CH3:11])=[C:4]([O:3][CH3:2])[CH:5]=3)[S:13](=[O:20])(=[O:21])[CH2:14][CH2:15][CH2:16][S:17]2(=[O:19])=[O:18])[CH:7]=[CH:8][C:9]=1[O:10][CH3:11]

Participants

3

Reactant 1

HCID 86734427HCID 86734427, compound

Product 1

HCID 86734426HCID 86734426, compound

Reagents, catalysts & solvents 1

HCID 21584569Ethylacetate acetoneSolvent

Procedure

2-(3,4-dimethoxyphenyl)-N-methyl-N-(p-methylphenethyl)-m-dithiane-2-propylamine-1,1,3,3-tetraoxide hydrochloride of melting point 169°-171° C (from acetone/ethyl acetate).

Sources & evidence

ORD record
ord-b14e0bd7ded54acba0a41ecaf8299fac
Source dataset
uspto-grants-1977_01
Patent number
US04003914

Reaction notes

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