HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 57268665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Nitroethane | HCID 6587 | — |
| Reactant | 2-Propen-1-one, 3-(4-chlorophenyl)-1-cyclopropyl- | HCID 4520528 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 57268665 | HCID 57268665 | — |
Reaction Steps
The procedure of Example IX using 24.3 g of 1-cyclopropyl-3-(p-chlorophenyl)prop-2-en-1-one, 11 ml of nitroethane and 1.5 g of sodium in 120 ml of methanol, gives 25 g of 1-cyclopropyl-3-(p-chlorophenyl)-4-nitropentanone as an oily residue which is used in the crude state for the remainder of the operations.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04005103 |
| Source dataset | uspto-grants-1977_01 |
| ORD ID | ord-94feced6d85d474f956a8137a8b47f6c |
| Source note | uspto-grants-1977_01 |